Nuclear Magnetic Spectroscopy

Anasazi NMR EM360 NMR Spectrometer

Miramar College's
AA240 Varian AAS

fid1H NMR Spectrum

Table of Content
   
1 Theory
2 Instrumentation
3 Basic Operation
4 Experiments
5 Interpreting Spectra
6 Animation and Multimedia
7 Literature

FID of NMR

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Theory
   
1 General Overiew
2 Basic Theory
3 NMR Spectroscopy
  NMR Spectroscopy, Kutztown Chemistry, Pennsylvania
  NMR Spectra and Spectroscopy
  Pulse Sequence

1H Nuclei

Nuclei in Magnetic Field

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Instrumentation
   
1 Anasazi EFT 60 MHz Spectrometer
a. College of Southern Idaho
b.
  Acorn NMR Inc, Software for Miramar NMR Spectrometer

Anasazi NMR Spectrometer

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Basic Operation
1 FGarces, SOP Guideline (Download and read before using spectrometer)
2

Running the Anasazi NMR Spectrometer
a Sample Prep
b Shimming
c. EFT Quick Guide
d. Nuts, NMR Utility Software
e.

3 Video Tutorial:
4 Sample Preparation 1 2 3 4 5 6 7 8
5 Shimming 1 2 3 4 5 6 7
6 Anasazi Operation, New Mexico State University SOP
7 Anasazi Broadband Operation
8 Anasazi Software Tutorial
   
   

Spectra from NUTS

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Experiments
   
1 1H NMR
2 13C NMR
3 2D NMR COSY, Wikipedia
4 Attached Proton Test Expeiments
5 DEPT and 13C NMR, Harvey Mudd Resource
6 HETCOR
  Relaxation Concepts, Wikipedia

NMR Recovery

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Spectra Interpretation
   
 

n+1 Rule for interpreting 1H NMR Spectra

Ethylmethylketone

Ethylmethylester

2-bromo-2-methyethanoic acid

1-bromo-2,2-dimethylpropane

Interpreting 2D NMR Spectra

 




1 n+1 Rule Interpreting NMR Spectra

2 Spek Teck 02 Spectra interpretation of methylethylketone

3 Spek Teck 03 Spectra interpretation of methylethylester

 
4 Spek Teck 08 Spectra interpretation of 2-bromo-2-methyethanoic acid

5 1H NMR Spectra interpretation of 1-bromo-2,2-dimethylpropane

 
6 Interpretation 2D NMR Spectra: COSY and HETCOR (PDF)

   


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Animations and Multimedia
   
1 How to run an NMR spctrometer and interpret an NMR spectrum.
2 .
   

2D COSY Spectra

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Literature
   
1 NMR Course from Queens University 
2 Introduction to NMR Series
3 Guide to Basic NMR, Northern Illinois University
4 Wiki NMR, Collection of NMR Experiments
5 Wikpedia NMR Spectroscopy
6 2D NMR Spectroscopy
7 Structure Elucidation via NMR

Spectra Series

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